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The first order of business is
setting up the CBL.
In this particular experiment I
chose to have the CBL collect and display temperature data
graphically every 5 seconds just to illustrate some of the
capabilities we will use later in the year. All we actually need
are the initial and final water temperatures.
50.0 mL of water were added to
the double-styrofoam cup calorimeter (HC = 5.0 J/oC).
Then the solids were massed into the test tube, taring after the
first solid. Since the reaction is very slow before mechanical
mixing, we don't need to worry about rushing. This same technique
was used, you may recall, in the zinc iodide experiment earlier
in the year. 0.75 g of the sodium sulfate decahydrate and 0.57 g
of the ammonium nitrate were used.
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